$ 608.99
Details
The Copper catalyzed amination kits is the ideal tools for the investigation of Ullmann reaction conditions. This enables to conveniently screen multiple reaction conditions simultaneously using pre-weighed catalysts and reagents. We offer pre-selected arrays of precatalysts and salts or custom arrays depending on your needs.Key variablesCopper Source: CuILigands: Phenanthroline, S-Proline, 1,2 cyclohexanediamine, N,N’dimethylethylenediamine, IsobutyrylcyclohexanoneBase: K2CO3, Cs2CO3 and K3PO4Solvent: DMF, DMSO, dioxane or acetonitrileTemperature: 40°C -> 120°CBenefitsFacilitates screen of reaction conditionsNo glove-box needed to manipulate air sensitive or moisture sensitive reagentsEnables up to 32 reaction conditions simultaneouslySave substrate using low scale reaction conditionsSave time on optimizationFeatures2 ml vial with screw cap and stirring bar.Specifically designed reaction blockPre-weighed reagents and catalystsTemperature from 0°C to 120°CPre-designed or custom arrays availableReagents are packaged under inert atmosphereStandard Protocol: 50 µmol of substrates in 500 µl solvent (DMF, DMSO, dioxane or acetonitrile, 0.1 mol/L concentration) with 0.1 equivalent of CuI, 0.2 equivalent of ligand and 1.1 equivalent of base.Kit contents: 2 reaction vials of each catalyst system and base, 36 reaction vials total
